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Beilstein J. Org. Chem. 2016, 12, 1493–1502, doi:10.3762/bjoc.12.146
Graphical Abstract
Scheme 1: Proposed routes for the three-component condensation [7].
Scheme 2: Synthetic methods for (aminomethylene)bisphosphonates I.
Scheme 3: Synthetic methods for (aminomethylene)bisphosphonates II.
Scheme 4: Synthetic methods for (aminomethylene)bisphosphine oxides.
Scheme 5: Synthesis of alkylamino- and (phenylaminomethylene)bisphosphine oxides.
Scheme 6: Synthesis of (dialkylaminomethylene)bisphosphine oxides.
Scheme 7: Synthesis of tetramethyl (phenylaminomethylene)bisphosphonate.
Scheme 8: Synthesis of (dialkylaminomethylene)bisphosphonates.
Figure 1: Effect of the quantity of dimethyl phosphite (DMP) on the product composition (from Table 6, entries 1–5.)
Figure 2: GC–MS chromatogram for the condensation of aniline, triethyl orthoformate and 2 equivalents of dime...
Figure 3: 31P NMR spectrum for the condensation of aniline, triethyl orthoformate and 2 equivalents of dibuty...